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Analytical Chemistry I
by Ulf RitgenThis workbook takes you through the successful work Harris, Textbook of Quantitative Analysis and is designed primarily for self-study. In five parts, the lecture content of analytical chemistry is summarized and explained using selected examples. Basic concepts of analytical chemistry are presented as well as the principle and various techniques of dimensional analysis and chromatography. UV/VIS, infrared and Raman spectroscopy are used to explain the investigation of molecularly present compounds, and selected techniques of atomic spectroscopy conclude the introduction to the fundamentals of analysis. The textbook's essential sections and illustrations are repeatedly referred to, which facilitates independent learning of the fundamentals of analytical chemistry.Easy to read, the book introduces the fundamentals and key techniques of analytical chemistry; it is aimed at undergraduate students of chemistry or related science subjects. It repeatedly refers back to the basics familiar from courses in general chemistry, so that the connections between what is already known and what is new become immediately apparent. Learning with this workbook has been tested in a distance learning chemistry course and facilitates preparation for module examinations in analytical chemistry.This book is a translation of the original German 1st edition Analytische Chemie I by Ulf Ritgen, published by Springer-Verlag GmbH Germany, part of Springer Nature in 2019. The translation was done with the help of artificial intelligence (machine translation by the service DeepL.com). A subsequent human revision was done primarily in terms of content, so that the book will read stylistically differently from a conventional translation. Springer Nature works continuously to further the development of tools for the production of books and on the related technologies to support the authors.
Analytical Chemistry II
by Ulf RitgenThis workbook takes you through the successful textbook Skoog/Holler/Crouch, Instrumentelle Analytik and is designed primarily for self-study.In five parts, the lecture content of more advanced analytical chemistry is summarized and explained using selected examples: mass spectrometry and nuclear magnetic resonance spectroscopy deal with the investigation of molecules, and numerous electroanalytical methods such as potentiometry, coulometry, amperometry and voltammetry are also covered. An overview of more specialized analytical methods includes the use of radioactive substances and various fluorescence methods, as well as methods of information acquisition in the increasingly important electrochemical and optical sensor technology and their automation. The course concludes with a summary of various principles and application methods of statistics, which are simply indispensable in the context of analytics. In order to facilitate independent learning, references to essential sections and illustrations of the textbook are made throughout the book.Not least because of the numerous examples, the book, which is aimed at students of chemistry or related scientific subjects, provides an easy-to-understand introduction to more complex aspects of analytical chemistry. In direct continuation of the workbook Analytical Chemistry I, references are made again and again to already known basics from other courses, which facilitate the linking of the familiar and the new. Learning with this workbook has been tested in a distance learning chemistry course and facilitates preparation for module examinations in more advanced analytical chemistry.This book is a translation of the original German 1st edition Analytische Chemie II by Ulf Ritgen, published by Springer-Verlag GmbH Germany, part of Springer Nature in 2020. The translation was done with the help of artificial intelligence (machine translation by the service DeepL.com). A subsequent human revision was done primarily in terms of content, so that the book will read stylistically differently from a conventional translation. Springer Nature works continuously to further the development of tools for the production of books and on the related technologies to support the authors.
Analytical Chemistry of Aerosols: Science and Technology
by Kvetoslav Rudolf SpurnyUntil the 1980s, researchers studied and measured only the physical properties of aerosols. Since the 80s, however, interest in the physicochemcal properties of aerosols has grown tremendously. Scientists in environmental hygiene, medicine, and toxicology have recognized the importance held by the chemical composition and properties of aerosols and the interactions of inhaled, "bad" aerosols.This book offers the first comprehensive treatment of modern aerosol analytical methods, sampling and separation procedures, and environmental applications, and offers critical reviews of the latest literature. This important field has developed rapidly in the last 15 years, but until now, no book effectively summarized or analyzed the existing research.Analytical Chemistry of Aerosols reviews procedures, techniques, and trends in the measurement and analysis of atmospheric aerosols. With contributions from acknowledged, international experts, the book discusses various methods of bulk analysis, single particle analysis, and the analysis of special aerosol systems, including fibrous and bacterial aerosols.
Analytical Chemistry of PCBs
by Mitchell D. EricksonThis updated and expanded Second Edition of Dr. Erickson's Analytical Chemistry of PCBs appears a decade after the first and is completely revised and updated. The changes from the First Edition reflect the significant growth in the area and a growing appreciation of the importance of PCB analysis to our culture. This book is a comprehensive review of the analytical chemistry of PCBs. It is part history, part annotated bibliography, part comparison, and part guidance. Featuring a new chapter on analyst/customer interactions and several new appendices, the Second Edition is an invaluable resource for both chemists with no experience in PCB analysis and seasoned PCB researchers. All topics have been more thoroughly treated and updated in this new edition to reflect advances made in the last decade, especially:
Analytical Chemistry of Uranium: Environmental, Forensic, Nuclear, and Toxicological Applications
by Zeev KarpasAccurate uranium analysis, and particularly for isotope measurements, is essential in many fields, including environmental studies, geology, hydrogeology, the nuclear industry, health physics, and homeland security. This volume covers the fascinating advances in the field of analytical chemistry of uranium. Exploring a broad range of topics, the book focuses on industrial processes that involve uranium, its presence in the environment, health and biological implications of exposure to uranium compounds, and nuclear forensics. Each chapter includes an overview of the topic and several examples to demonstrate the analytical procedures. Separation and purification techniques are included where necessary.
Analytical Chemistry Refresher Manual
by John KenkelAnalytical Chemistry Refresher Manual provides a comprehensive refresher in techniques and methodology of modern analytical chemistry. Topics include sampling and sample preparation, solution preparation, and discussions of wet and instrumental methods of analysis; spectrometric techniques of UV, vis, and IR spectroscopy; NMR, mass spectrometry, and atomic spectrometry techniques; analytical separations, including liquid-liquid extraction, liquid-solid extraction, instrumental and non-instrumental chromatography, and electrophoresis; and basic theory and instrument design concepts of gas chromatography and high-performance liquid chromatography. The manual also covers automation, potentiometric and voltammetric techniques, and the detection and accounting of laboratory errors. Analytical Chemistry Refresher Manual will benefit all laboratory workers, water and wastewater professionals, and academic researchers who are looking for a readable reference covering the fundamentals of modern analytical chemistry.
Analytical Design of PID Controllers
by Iván D. Díaz-Rodríguez Sangjin Han Shankar P. BhattacharyyaThis monograph presents a new analytical approach to the design of proportional-integral-derivative (PID) controllers for linear time-invariant plants. The authors develop a computer-aided procedure, to synthesize PID controllers that satisfy multiple design specifications. A geometric approach, which can be used to determine such designs methodically using 2- and 3-D computer graphics is the result.The text expands on the computation of the complete stabilizing set previously developed by the authors and presented here. This set is then systematically exploited to achieve multiple design specifications simultaneously. These specifications include classical gain and phase margins, time-delay tolerance, settling time and H-infinity norm bounds. The results are developed for continuous- and discrete-time systems. An extension to multivariable systems is also included.Analytical Design of PID Controllers provides a novel method of designing PID controllers, which makes it ideal for both researchers and professionals working in traditional industries as well as those connected with unmanned aerial vehicles, driverless cars and autonomous robots.
Analytical Electrochemistry
by Joseph WangANALYTICAL ELECTROCHEMISTRY An accessible and robust text with comprehensive coverage of modern electroanalytical techniques and devices In the newly revised 4th edition of Analytical Electrochemistry, distinguished researcher Dr. Joseph Wang delivers an authoritative and comprehensive discussion of modern electroanalytical techniques and devices. With a strong focus on electroanalysis (as opposed to physical electrochemistry), the book offers readers a thorough grounding in the fundamentals of electrode reactions and the principles of electrochemical methods. It also demonstrates the solving of real-life analytical problems using the techniques discussed within. This latest edition contains extensive updates to the cited literature and its descriptions of various electrochemical processes and techniques. Additional worked examples are included in the text and numerous quantitative questions and exercise problems are found at the end of each chapter. Readers will also find: A thorough introduction to the fundamental concepts of electroanalysis, including discussions of Faradaic processes, electrical double layers, and the electrocapillary effect Comprehensive explorations of the study of electrode reactions, interfacial properties, and controlled potential techniques Practical discussions of the practical considerations of electroanalysis, including electrochemical cells, solvents and supporting electrolytes, and instrumentation Detailed treatments of potentiometry and electrochemical sensors, including ion selective electrodes, electrochemical biosensors and wearable devices Perfect for graduate students studying electroanalytical chemistry, Analytical Electrochemistry will also benefit advanced undergraduate students taking courses in instrumental analysis, as well as academics and industrial professionals considering the use of electroanalysis in their labs.
Analytical Estimates of Structural Behavior
by Clive L. Dym Harry E. WilliamsExplicitly reintroducing the idea of modeling to the analysis of structures, Analytical Estimates of Structural Behavior presents an integrated approach to modeling and estimating the behavior of structures. With the increasing reliance on computer-based approaches in structural analysis, it is becoming even more important for structural engineers
Analytical Food Microbiology: A Laboratory Manual
by Ahmed E. Yousef Joy G. Waite-Cusic Jennifer J. PerryThe new edition of the highly regarded laboratory manual for courses in food microbiology Analytical Food Microbiology: A Laboratory Manual develops the practical skills and knowledge required by students and trainees to assess the microbiological quality and safety of food. This user-friendly textbook covers laboratory safety, basic microbiological techniques, evaluation of food for various microbiological groups, detection and enumeration of foodborne pathogens, and control of undesirable foodborne microorganisms. Each well-defined experiment includes clear learning objectives and detailed explanations to help learners understand essential techniques and approaches in applied microbiology. The fully revised second edition presents improved conventional techniques, advanced analytical methodologies, updated content reflecting emerging food safety concerns, and new laboratory experiments incorporating commercially available microbiological media. Throughout the book, clear and concise chapters explain culture- and molecular-based approaches for assessing microbial quality and safety of diverse foods. This expanded and updated resource: Reviews aseptic techniques, dilution, plating, streaking, isolation, and other basic microbiological procedures Introduces exercises and relevant microorganisms with pertinent background information and reference material Describes each technique using accessible explanatory text, detailed illustrations, and easy-to-follow flowcharts Employs a proven “building block” approach throughout, with each new chapter building upon skills from the previous chapter Provides useful appendices of microbiological media, recommended control organisms, available supplies and equipment, and laboratory exercise reports With methods drawn from the authors’ extensive experience in academic, regulatory, and industry laboratories, Analytical Food Microbiology: A Laboratory Manual, Second Edition, is ideal for undergraduate and graduate students in food microbiology courses, as well as food processors and quality control personnel in laboratory training programs.
Analytical Groundwater Modeling: Theory and Applications using Python
by Mark Bakker Vincent PostThis book provides a detailed description of how Python can be used to give insight into the flow of groundwater based on analytic solutions. Starting with simple problems to illustrate the basic principles, complexity is added step by step to show how one-dimensional and two-dimensional models of one or two aquifers can be implemented. Steady and transient flow problems are discussed in confined, semi-confined, and unconfined aquifers that may include wells, rivers, and areal recharge. Special consideration is given to coastal aquifers, including the effect of tides and the simulation of interface flow. Application of Python allows for compact and readable code, and quick visualization of the solutions. Python scripts are provided to reproduce all results. The scripts are also available online so that they can be altered to meet site-specific conditions. This book is intended both as training material for the next generation of university students and as a useful resource for practitioners. A primer is included for those who are new to Python or as a refresher for existing users.
Analytical Heat and Fluid Flow in Microchannels and Microsystems (Mechanical Engineering Series)
by Renato M. Cotta Diego C. Knupp Carolina P. Naveira-CottaThis book focuses on the modeling and analysis of heat and fluid flow in microchannels and micro-systems, compiling a number of analytical and hybrid numerical-analytical solutions for models that account for the relevant micro-scale effects, with the corresponding experimental analysis validation when applicable. The volume stands as the only available compilation of easy to use analytically-based solutions for micro-scale heat and fluid flow problems, that systematically incorporates the most relevant micro-scale effects into the mathematical models, followed by their physical interpretation on the micro-system behavior.
Analytical Heat Transfer
by Je-Chin HanFilling the gap between basic undergraduate courses and advanced graduate courses, this text explains how to analyze and solve conduction, convection, and radiation heat transfer problems analytically. It describes many well-known analytical methods and their solutions, such as Bessel functions, separation of variables, similarity method, integral method, and matrix inversion method. Developed from the author's 30 years of teaching, the text also presents step-by-step mathematical formula derivations, analytical solution procedures, and numerous demonstration examples of heat transfer applications.
Analytical Heat Transfer
by Je-Chin Han Lesley M. WrightAnalytical Heat Transfer explains how to analyze and solve conduction, convection, and radiation heat transfer problems. It enables students to tackle complex engineering heat transfer problems prevalent in practice. Covering heat transfer in high-speed flows and unsteady highly turbulent flows, the book also discusses enhanced heat transfer in channels, heat transfer in rotating channels, numerical modeling for turbulent flow heat transfer, and thermally developing heat transfer in a circular tube. The second edition features new content on Duhamel’s superposition method, Green’s function method for transient heat conduction, finite-difference method for steady state and transient heat conduction in cylindrical coordinates, and laminar mixed convection. It includes two new chapters on laminar-to-turbulent transitional heat transfer and turbulent flow heat transfer enhancement, in addition to end-of-chapter problems. The book bridges the gap between basic heat transfer undergraduate courses and advanced heat transfer graduate courses for a single semester of intermediate heat transfer, advanced conduction/radiation heat transfer, or convection heat transfer. Features: Focuses on analyzing and solving classic heat transfer problems in conduction, convection, and radiation Covers 2-D and 3-D view factor evaluation, combined radiation with conduction and/or convection, and gas radiation optically thin and optically thick limits Features updated content and new chapters on mass and heat transfer analogy, thermally developing heat transfer in a circular tube, laminar-turbulent transitional heat transfer, unsteady highly turbulent flows, enhanced heat transfer in channels, heat transfer in rotating channels, and numerical modeling for turbulent flow heat transfer Provides step-by-step mathematical formula derivations, analytical solution procedures, and demonstration examples Includes end-of-chapter problems with an accompanying Solutions Manual for instructors This book is ideal for undergraduate and graduate students studying basic heat transfer and advanced heat transfer.
Analytical Imaging Techniques for Soft Matter Characterization (Engineering Materials)
by Vikas Mittal Nadejda B. MatskoThe book aims to describe the microscopic characterization of the soft matter in the light of new advances acquired in the science of microscopy techniques like AFM; SEM; TEM etc. It does not focus on the traditional information on the microscopy methods as well as systems already present in different books, but intends to answer more fundamental questions associated with commercially important systems by using new advances in microscopy. Such questions are generally not answered by other techniques. The contents of the book also reflect this as the chapters are not based on describing only material systems, but are based on the answering the problems or questions arising in their characterization. Both qualitative as well as quantitative analysis using such microscopic techniques is discussed. Moreover, efforts have been made to provide a broader reach as discussions on both polymers as well as biological matter have been included as different sections. Such a text with comprehensive overview of the various characterization possibilities using microscopy methods can serve as a valuable reference for microscopy experts as well as non-experts alike
Analytical Measurements in Aquatic Environments (Analytical Chemistry)
by Jacek Namieśnik Piotr SzeferEven a cursory perusal of any analytical journal will demonstrate the increasing important of trace and ultra-trace analysis. And as instrumentation continues to develop, the definition of the term "trace element" will undoubtedly continue to change. Covering the composition and underlying properties of freshwater and marine systems, Analytical Mea
Analytical Mechanics
by Louis N. Hand Janet D. FinchAnalytical Mechanics, first published in 1999, provides a detailed introduction to the key analytical techniques of classical mechanics, one of the cornerstones of physics. It deals with all the important subjects encountered in an undergraduate course and prepares the reader thoroughly for further study at graduate level. The authors set out the fundamentals of Lagrangian and Hamiltonian mechanics early on in the book and go on to cover such topics as linear oscillators, planetary orbits, rigid-body motion, small vibrations, nonlinear dynamics, chaos, and special relativity. A special feature is the inclusion of many 'e-mail questions', which are intended to facilitate dialogue between the student and instructor. Many worked examples are given, and there are 250 homework exercises to help students gain confidence and proficiency in problem-solving. It is an ideal textbook for undergraduate courses in classical mechanics, and provides a sound foundation for graduate study.
Analytical Mechanics (Undergraduate Lecture Notes in Physics)
by Carl S. HelrichThis advanced undergraduate textbook begins with the Lagrangian formulation of Analytical Mechanics and then passes directly to the Hamiltonian formulation and the canonical equations, with constraints incorporated through Lagrange multipliers. Hamilton's Principle and the canonical equations remain the basis of the remainder of the text. Topics considered for applications include small oscillations, motion in electric and magnetic fields, and rigid body dynamics. The Hamilton-Jacobi approach is developed with special attention to the canonical transformation in order to provide a smooth and logical transition into the study of complex and chaotic systems. Finally the text has a careful treatment of relativistic mechanics and the requirement of Lorentz invariance. The text is enriched with an outline of the history of mechanics, which particularly outlines the importance of the work of Euler, Lagrange, Hamilton and Jacobi. Numerous exercises with solutions support the exceptionally clear and concise treatment of Analytical Mechanics.
Analytical Mechanics
by Nivaldo A. LemosAnalytical mechanics is the foundation of many areas of theoretical physics including quantum theory and statistical mechanics, and has wide-ranging applications in engineering and celestial mechanics. This introduction to the basic principles and methods of analytical mechanics covers Lagrangian and Hamiltonian dynamics, rigid bodies, small oscillations, canonical transformations and Hamilton–Jacobi theory. This fully up-to-date textbook includes detailed mathematical appendices and addresses a number of advanced topics, some of them of a geometric or topological character. These include Bertrand's theorem, proof that action is least, spontaneous symmetry breakdown, constrained Hamiltonian systems, non-integrability criteria, KAM theory, classical field theory, Lyapunov functions, geometric phases and Poisson manifolds. Providing worked examples, end-of-chapter problems, and discussion of ongoing research in the field, it is suitable for advanced undergraduate students and graduate students studying analytical mechanics.
An Analytical Mechanics Framework for Flow-Oscillator Modeling of Vortex-Induced Bluff-Body Oscillations (Solid Mechanics and Its Applications #260)
by Sohrob Mottaghi Rene Gabbai Haym BenaroyaThis self-contained book provides an introduction to the flow-oscillator modeling of vortex-induced bluff-body oscillations. One of the great challenges in engineering science also happens to be one of engineering design – the modeling, analysis and design of vibrating structures driven by fluid motion. The literature on fluid–structure interaction is vast, and it can be said to comprise a large fraction of all papers published in the mechanical sciences. This book focuses on the vortex-induced oscillations of an immersed body, since, although the importance of the subject has long been known, it is only during the past fifty years that there have been concerted efforts to analytically model the general behavior of the coupling between vortex shedding and structural oscillations. At the same time, experimentalists have been gathering data on such interactions in order to help define the various regimes of behavior. This data is critical to our understanding and to those who develop analytical models, as can be seen in this book. The fundamental bases for the modeling developed in this book are the variational principles of analytical dynamics, in particular Hamilton’s principle and Jourdain’s principle, considered great intellectual achievements on par with Newton’s laws of motion. Variational principles have been applied in numerous disciplines, including dynamics, optics and quantum mechanics. Here, we apply variational principles to the development of a framework for the modeling of flow-oscillator models of vortex-induced oscillations.
Analytical Mechanics (Seventh Edition)
by Grant R. Fowles George L. CassidayThis textbook is intended for an undergraduate course in classical mechanics taken by students majoring in physics, physical science, or engineering.
Analytical Method Development and Validation
by Michael Swartz Ira S. KrullDescribes analytical methods development, optimization and validation, and provides examples of successful methods development and validation in high-performance liquid chromatography (HPLC) areas. The text presents an overview of Food and Drug Administration (FDA)/International Conference on Harmonization (ICH) regulatory guidelines, compliance with validation requirements for regulatory agencies, and methods validation criteria stipulated by the US Pharmacopia, FDA and ICH.
Analytical Methodologies for Biofilm Research (Springer Protocols Handbooks)
by Moupriya Nag Dibyajit LahiriThe book provides the readers of various discipline an easy understanding of the latest biophysical techniques pertaining to microbiology. Biofilm associated chronic infection is a major health problem and a serious concern to doctors, scientists and other health workers as it develops antibiotic and multi-drug resistance. This book describes various protocols utilized in the detection of the biofilm. The book has been divided into six sub sections which provides pertinent information about the various biophysical techniques and instruments that are used for detecting and analyzing the biofilm formation upon biotic and abiotic surfaces. The readers will be able to identify the techniques that can best cater information to solve the problem at hand. This book attempts to compile the latest information on the recent advances in the various functional aspects of microbial biofilms, their pathogenesis, present day treatments as well as detection strategies.This book is meant for researchers in the field of microbiology and interested in understanding microbial pathogenesis, quorum sensing and biofilm formation.
Analytical Methods and Instruments for Micro- and Nanomaterials (Lecture Notes in Nanoscale Science and Technology #23)
by Henry H. Radamson Anders Hallén Ilya Sychugov Alexander AzarovThis book describes analytical instruments widely used to characterize the nanostructured materials. It provides information about how to assess material quality, defects, the state of surfaces and interfaces, element distributions, strain, lattice distortion, and electro-optical properties of materials and devices. The information provided by this book can be used as a back-up for material processing, material design and debugging of device performance. The basic principles and methodology of each analysis technique is described in separate chapters, adding historic perspectives and recent developments. The data analysis, from simple to advanced level, is introduced by numerous examples, mostly taken from the authors' fields of research; semiconductor materials, metals and oxides. The book serves as a valuable guide for scientists and students working in materials science, physics, and engineering, who wish to become acquainted with the most important analytical techniques for nanomaterials.
Analytical Methods for Environmental Contaminants of Emerging Concern
by Núria Fontanals Rosa Maria MarcéAnalytical Methods for Environmental Contaminants of Emerging Concern Provides the analytical methodology required to detect different families of organic compounds of emerging concern (CECs) from environmental samples Most contaminants of emerging concern (CECs) —such as pharmaceuticals, personal care products, pesticides, sunscreens, perfluorinated compounds, and microplastics—have been present in the environment for years, yet some have only recently been identified, and many of these organic compounds remain unregulated. Analytical methods have been developed to determine the toxicity and risk of different families of CECs. Analytical Methods for Environmental Contaminants of Emerging Concern presents the methods currently available to determine families of organic CECs in environmental samples. Each section of the book is devoted to a particular family of CECs, covering different analytical methods supported by examples of both cutting-edge research and commonly used methods. An international panel of experts describes every step of the analytical procedures, including sample preparation, chromatographic separation coupled to mass spectrometry or other instrumental techniques. Specific requirements are linked to the properties of the contaminants and the sample matrix for each procedure presented. Throughout the book, in-depth case studies of analytical procedures for CEC extraction, separation, and determination are presented to help readers transfer the analytical methods to their laboratories. Provides detailed descriptions of various approaches for determining each group of CECs in environmental samples Covers different types of aqueous, solid, and atmospheric samples Includes up-to-date information on CEC properties, relevant legislation, reported or potential metabolites/transformation products, and environmental occurrence Addresses CECs such as novel psychoactive substances, artificial sweeteners, musk fragrances, disinfection byproducts, and microplastics Offers practical tips and advice on special care procedures to assist readers in CEC determination Analytical Methods for Environmental Contaminants of Emerging Concern is an essential reference and guide for advanced students and researchers in analytical chemistry and science, environmental science, forensic science, and specialized subjects related to analytical chemistry.