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Solid Oxide Fuel Cells: From Fundamental Principles to Complete Systems
by Radenka MaricSolid Oxide Fuel Cells: From Fundamental Principles to Complete Systems is as a valuable resource for beginners, experienced researchers, and developers of solid oxide fuel cells. It provides a fundamental understanding of SOFCs by covering the present state-of-the-art as well as ongoing research and future challenges to be solved. It discusses current and future materials and provides an overview of development activities with a more general system approach toward fuel cell plant technology, including plant design and economics, industrial data and advances in technology. Provides an understanding of the operating principles of SOFCs Discusses state-of-the-art materials, technologies and processes Includes a review of current industry and lessons learned Offers a more general system approach toward fuel cell plant technology, including plant design and economics of SOFC manufacture Covers significant technical challenges that remain to be solved Presents the status of government activities, industry and market This book is aimed at electrochemists, batteries and fuel cell engineers, alternative energy scientists, and professionals in materials science.
Solid Oxide Fuels Cells: Facts and Figures
by John T.S. Irvine Paul ConnorSolid Oxide Fuel Cells (SOFCs) operate at high temperatures allowing more fuel flexibility and also useful heat output and so increase total efficiency, but does give some interesting engineering challenges. Solid Oxide Fuels Cells: Facts and Figures provides clear and accurate data for a selection of SOFC topics from the specific details of Ni cermet anodes, chemical expansion in materials, and the measuring and modelling of mechanical stresses, to the broader scope of the history and present design of cells, to SOFC systems and the future of SOFC. Celebrating Ulf Bossel's work on Solid Oxide Fuel Cells, and especially his running of the European Fuel Cell Forum, Solid Oxide Fuels Cells: Facts and Figures covers important topics on the way including intermediate temperature fuel cells, metal supported fuel cells and both new materials and engineering solutions to some of the challenges of getting SOFC to market. The chapters are based on the special plenary talks given by some of the most respected and talented people in the field at the 2010 European SOFC Forum in Luzern and the title for this book comes from the report produced by Ulf for the IEA "Final Report on SOFC Data, Facts and Figures", Swiss Federal Office of Energy, Berne, 1992. The comprehensive nature of Solid Oxide Fuels Cells: Facts and Figures makes it a key resource of SOFC topics for students, lecturers, researchers and industry practitioners alike.
Solid Phase Microextraction
by Gangfeng Ouyang Ruifen JiangThis book offers comprehensive information on the developments and applications of the solid phase microextraction (SPME) technique. The first part of the book briefly introduces readers to the fundamentals of SPME, while subsequent sections describe the applications of SPME technique in detail, including environmental analysis (air, water, soil/sediments), food analysis (volatile/nonvolatile compounds), and bioanalysis (plants, animal tissues, body fluids). The advantages and future challenges of the SPME technique are also discussed. Including recent research advances and further developments of SPME, the book offers a practical reference guide and a valuable resource for researchers and users of SPME techniques. The target audience includes analytical chemists, environmental scientists, biological scientists, material scientists, and analysts, as well as students at universities/institutes in related fields. Dr. Gangfeng Ouyang is a Professor at the School of Chemistry and Chemical Engineering, Sun Yat-sen University, China. Dr. Ruifen Jiang is an Associate Professor at the School of Environment, Jinan University, China.
Solid-Phase Organic Syntheses, Solid-Phase Palladium Chemistry
by Peter J. ScottIntegrates solid-phase organic synthesis with palladium chemistryThe Wiley Series on Solid-Phase Organic Syntheses keeps researchers current with major accomplishments in solid-phase organic synthesis, providing full experimental details. Following the validated, tested, and proven experimental procedures, readers can easily perform a broad range of complex syntheses needed for their own experiments and industrial applications. The series is conveniently organized into themed volumes according to the specific type of synthesis.This second volume in the series focuses on palladium chemistry in solid-phase synthesis, exploring palladium catalysts and reactions, procedures for preparation and utilization, ligands, and linker reactions. The first part of the volume offers a comprehensive overview of the field. Next, the chapters are organized into three parts:Part Two: Palladium-Mediated Solid-Phase Organic SynthesesPart Three: Immobilized Catalysts and LigandsPart Four: Palladium-Mediated Multifunctional CleavageEach chapter is written by one or more leading international experts in palladium chemistry. Their contributions reflect a thorough examination and review of the current literature as well as their own first-hand laboratory experience. References at the end of each chapter serve as a gateway to the field's literature.The introduction of palladium-mediated, cross-coupling reactions more than thirty years ago revolutionized the science of carbon-carbon bond formation. It has now become a cornerstone of today's synthetic organic chemistry laboratory. With this volume, researchers in organic and medicinal chemistry have access to a single resource that explains the fundamentals of palladium chemistry in solid-phase synthesis and sets forth clear, step-by-step instructions for conducting their own syntheses.
Solid-Phase Organic Synthesis
by Patrick H. Toy Yulin LamPresents both the fundamental concepts and the most recent applications in solid-phase organic synthesis With its emphasis on basic concepts, Solid-Phase Organic Synthesis guides readers through all the steps needed to design and perform successful solid-phase organic syntheses. The authors focus on the fundamentals of heterogeneous supports in the synthesis of organic molecules, explaining the use of a solid material to facilitate organic synthesis. This comprehensive text not only presents the fundamentals, but also reviews the most recent research findings and applications, offering readers everything needed to conduct their own state-of-the-art science experiments. Featuring chapters written by leading researchers in the field, Solid-Phase Organic Synthesis is divided into two parts: Part One, Concepts and Strategies, discusses the linker groups used to attach the synthesis substrate to the solid support, colorimetric tests to identify the presence of functional groups, combinatorial synthesis, and diversity-oriented synthesis. Readers will discover how solid-phase synthesis is currently used to facilitate the discovery of new molecular functionality. The final chapter discusses how using a support can change or increase reaction selectivity. Part Two, Applications, presents examples of the solid-phase synthesis of various classes of organic molecules. Chapters explore general asymmetric synthesis on a support, strategies for heterocyclic synthesis, and synthesis of radioactive organic molecules, dyes, dendrimers, and oligosaccharides. Each chapter ends with a set of conclusions that underscore the key concepts and methods. References in each chapter enable readers to investigate any topic in greater depth. With its presentation of basic concepts as well as recent findings and applications, Solid-Phase Organic Synthesis is the ideal starting point for students and researchers in organic, medicinal, and combinatorial chemistry who want to take full advantage of current solid-phase synthesis techniques.
Solid-Phase Synthesis of Nitrogenous Heterocycles (Topics in Heterocyclic Chemistry #52)
by Viktor KrchňákThe series Topics in Heterocyclic Chemistry presents critical reviews on present and future trends in the research of heterocyclic compounds. Overall the scope is to cover topics dealing with all areas within heterocyclic chemistry, both experimental and theoretical, of interest to the general heterocyclic chemistry community. The series consists of topic related volumes edited by renowned editors with contributions of experts in the field. All chapters from Topics in Heterocyclic Chemistry are published Online First with an individual DOI. In references, Topics in Heterocyclic Chemistry is abbreviated as Top Heterocycl Chem and cited as a journal.
Solid State Batteries: Design, Challenges and Market Demands (Advances in Material Research and Technology)
by Nithyadharseni Palaniyandy K. P. Abhilash B. NaliniThis book offers a comprehensive analysis of novel design strategies in higher energy solid-state lithium batteries. It describes synthesis and experimental techniques to characterize the physical, chemical and electrochemical properties of the electrode and electrolytes. The book reports on electrochemical measurements of conductivity and related parameters in solid electrolytes and its interfaces. It also presents various technologies that have been used for the fabrication of all-solid-state lithium-ion batteries such as thin-film, 3D printing (additive manufacturing) and atomic layer deposition. A large part of the text focus on the description on the complete functioning and challenges with the electrochemistry of the electrodes and solid electrolyte interfaces. The book also supplies valuable insight into potential growth opportunities in this exciting market and cost-effective design tactics in solid-state assemblies.
Solid State Characterization of Pharmaceuticals
by Ingvar Ymén Richard A. StoreyThe field of solid state characterization is central to the pharmaceutical industry, as drug products are, in an overwhelming number of cases, produced as solid materials. Selection of the optimum solid form is a critical aspect of the development of pharmaceutical compounds, due to their ability to exist in more than one form or crystal structure (polymorphism). These polymorphs exhibit different physical properties which can affect their biopharmaceutical properties.This book provides an up-to-date review of the current techniques used to characterize pharmaceutical solids. Ensuring balanced, practical coverage with industrial relevance, it covers a range of key applications in the field. The following topics are included: Physical properties and processesThermodynamicsIntellectual guidanceX-ray diffractionSpectroscopy MicroscopyParticle sizingMechanical propertiesVapour sorptionThermal analysis & CalorimetryPolymorph predictionForm selection
Solid State Chemistry: An Introduction
by Elaine A. Moore Lesley E. Smart"A comprehensive guide to solid-state chemistry which is ideal for all undergraduate levels. It covers well the fundamentals of the area, from basic structures to methods of analysis, but also introduces modern topics such as sustainability." Dr. Jennifer Readman, University of Central Lancashire, UK "The latest edition of Solid State Chemistry combines clear explanations with a broad range of topics to provide students with a firm grounding in the major theoretical and practical aspects of the chemistry of solids." Professor Robert Palgrave, University College London, UK Building a foundation with a thorough description of crystalline structures, this fifth edition of Solid State Chemistry: An Introduction presents a wide range of the synthetic and physical techniques used to prepare and characterise solids. Going beyond this, this largely nonmathematical introduction to solid-state chemistry includes the bonding and electronic, magnetic, electrical, and optical properties of solids. Solids of particular interest—porous solids, superconductors, and nanostructures—are included. Practical examples of applications and modern developments are given. It offers students the opportunity to apply their knowledge in real-life situations and will serve them well throughout their degree course. New in the Fifth Edition A new chapter on sustainability in solid-state chemistry written by an expert in this field Cryo-electron microscopy X-ray photoelectron spectroscopy (ESCA) Covalent organic frameworks Graphene oxide and bilayer graphene Elaine A. Moore studied chemistry as an undergraduate at Oxford University and then stayed on to complete a DPhil in theoretical chemistry with Peter Atkins. After a two-year postdoctoral position at the University of Southampton, she joined the Open University in 1975, becoming a lecturer in chemistry in 1977, senior lecturer in 1998, and reader in 2004. She retired in 2017 and currently has an honorary position at the Open University. She has produced OU teaching texts in chemistry for courses at levels 1, 2, and 3 and written texts in astronomy at level 2 and physics at level 3. She was team leader for the production and presentation of an Open University level 2 chemistry module delivered entirely online. She is a Fellow of the Royal Society of Chemistry and a Senior Fellow of the Higher Education Academy. She was co-chair for the successful Departmental submission of an Athena Swan bronze award. Lesley E. Smart studied chemistry at Southampton University, United Kingdom. After completing a PhD in Raman spectroscopy, she moved to a lectureship at the (then) Royal University of Malta. After returning to the United Kingdom, she took an SRC Fellowship to Bristol University to work on X-ray crystallography. From 1977 to 2009, she worked at the Open University chemistry department as a lecturer, senior lecturer, and Molecular Science Programme director, and she held an honorary senior lectureship there until her death in 2016. At the Open University, she was involved in the production of undergraduate courses in inorganic and physical chemistry and health sciences. She served on the Council of the Royal Society of Chemistry and as the chair of their Benevolent Fund.
Solid State Chemistry and its Applications
by Anthony R. WestSOLID STATE CHEMISTRY AND ITS APPLICATIONS A comprehensive treatment of solid state chemistry complete with supplementary material and full colour illustrations from a leading expert in the field. Solid State Chemistry and its Applications, Second Edition delivers an advanced version of West’s classic text in solid state chemistry, expanding on the undergraduate Student Edition to present a comprehensive treatment of solid state chemistry suitable for advanced students and researchers. The book provides the reader with an up-to-date account of essential topics in solid state chemistry and recent developments in this rapidly developing field of inorganic chemistry. Significant updates and new content in this second edition include: A more extensive overview of important families of inorganic solids including spinels, perovskites, pyrochlores, garnets, Ruddlesden-Popper phases and many more New methods to synthesise inorganic solids, including sol-gel methods, combustion synthesis, atomic layer deposition, spray pyrolysis and microwave techniques Advances in electron microscopy, X-ray and electron spectroscopies New developments in electrical properties of materials, including high Tc superconductivity, lithium batteries, solid oxide fuel cells and smart windows Recent developments in optical properties, including fibre optics, solar cells and transparent conducting oxides Advances in magnetic properties including magnetoresistance and multiferroic materials Homogeneous and heterogeneous ceramics, characterization using impedance spectroscopy Thermoelectric materials, MXenes, low dimensional structures, memristors and many other functional materials Expanded coverage of glass, including metallic and fluoride glasses, cement and concrete, geopolymers, refractories and structural ceramics Overview of binary oxides of all the elements, their structures, properties and applications Featuring full color illustrations throughout, readers will also benefit from online supplementary materials including access to CrystalMaker® software and over 100 interactive crystal structure models. Perfect for advanced students seeking a detailed treatment of solid state chemistry, this new edition of Solid State Chemistry and its Applications will also earn a place as a desk reference in the libraries of experienced researchers in chemistry, crystallography, physics, and materials science.
Solid State Chemistry and its Applications
by Anthony R. WestSolid State Chemistry and its Applications, 2nd Edition: Student Edition is an extensive update and sequel to the bestselling textbook Basic Solid State Chemistry, the classic text for undergraduate teaching in solid state chemistry worldwide.Solid state chemistry lies at the heart of many significant scientific advances from recent decades, including the discovery of high-temperature superconductors, new forms of carbon and countless other developments in the synthesis, characterisation and applications of inorganic materials. Looking forward, solid state chemistry will be crucial for the development of new functional materials in areas such as energy, catalysis and electronic materials.This revised edition of Basic Solid State Chemistry has been completely rewritten and expanded to present an up-to-date account of the essential topics and recent developments in this exciting field of inorganic chemistry. Each section commences with a gentle introduction, covering basic principles, progressing seamlessly to a more advanced level in order to present a comprehensive overview of the subject. This new Student Edition includes the following updates and new features:Expanded coverage of bonding in solids, including a new section on covalent bonding and more extensive treatment of metallic bonding.Synthetic methods are covered extensively and new topics include microwave synthesis, combinatorial synthesis, mechano-synthesis, atomic layer deposition and spray pyrolysis.Revised coverage of electrical, magnetic and optical properties, with additional material on semiconductors, giant and colossal magnetoresistance, multiferroics, LEDs, fibre optics and solar cells, lasers, graphene and quasicrystals.Extended chapters on crystal defects and characterisation techniques.Published in full colour to aid comprehension.Extensive coverage of crystal structures for important families of inorganic solids is complemented by access to CrystalMaker® visualization software, allowing readers to view and rotate over 100 crystal structures in three dimensions.Solutions to exercises and supplementary lecture material are available online.Solid State Chemistry and its Applications, 2nd Edition: Student Edition is a must-have textbook for any undergraduate or new research worker studying solid state chemistry.
Solid State Composites and Hybrid Systems: Fundamentals and Applications
by Rada Savkina Larysa KhomenkovaSolid state composites and hybrid systems offer multifunctional applications in various fields of human life, demonstrating solutions to the key problems of the environment, human health, biology, medicine, electronics, energy harvesting and storage. Exploring this innovative field of research, this book details the wide range of materials, techniques, and approaches utilised in composite and hybrid structures in recent years. It will be of interest not only for experienced researchers but also for postgraduate students and young researchers entering the fields of nanoscience, material sciences, and bioengineering. Features: Contains the latest research developments in the materials, techniques, patents, and approaches in the field Includes both fundamental aspects and applied research Edited by two highly experienced researchers
Solid State Development and Processing of Pharmaceutical Molecules: Salts, Cocrystals, and Polymorphism (Methods & Principles in Medicinal Chemistry)
by Raimund Mannhold Helmut Buschmann Jörg HolenzA guide to the latest industry principles for optimizing the production of solid state active pharmaceutical ingredients Solid State Development and Processing of Pharmaceutical Molecules is an authoritative guide that covers the entire pharmaceutical value chain. The authors—noted experts on the topic—examine the importance of the solid state form of chemical and biological drugs and review the development, production, quality control, formulation, and stability of medicines. The book explores the most recent trends in the digitization and automation of the pharmaceutical production processes that reflect the need for consistent high quality. It also includes information on relevant regulatory and intellectual property considerations. This resource is aimed at professionals in the pharmaceutical industry and offers an in-depth examination of the commercially relevant issues facing developers, producers and distributors of drug substances. This important book: Provides a guide for the effective development of solid drug forms Compares different characterization methods for solid state APIs Offers a resource for understanding efficient production methods for solid state forms of chemical and biological drugs Includes information on automation, process control, and machine learning as an integral part of the development and production workflows Covers in detail the regulatory and quality control aspects of drug development Written for medicinal chemists, pharmaceutical industry professionals, pharma engineers, solid state chemists, chemical engineers, Solid State Development and Processing of Pharmaceutical Molecules reviews information on the solid state of active pharmaceutical ingredients for their efficient development and production.
Solid State Electrochemistry II: Electrodes, Interfaces and Ceramic Membranes
by Vladislav V. KhartonThe ideal addition to the companion volume on fundamentals, methodologies, and applications, this second volume combines fundamental information with an overview of the role of ceramic membranes, electrodes and interfaces in this important, interdisciplinary and rapidly developing field. Written primarily for specialists working in solid state electrochemistry, this first comprehensive handbook on the topic focuses on the most important developments over the last decade, as well as the methodological and theoretical aspects and practical applications. This makes the contents equally of interest to material, physical and industrial scientists, and to physicists. Also available as a two-volume set.
Solid State Fermentation: Research and Industrial Applications (Advances in Biochemical Engineering/Biotechnology #169)
by Susanne Steudler Anett Werner Jay J. ChengThis book reviews the wide range of products and applications of solid state fermentation as well as the development of this cultivation technology over the last years. In this book, readers will also learn about the challenges of solid state fermentation, including process management, reactor design, scale-up and the formation of process-specific products. Solid fermentation is a traditional cultivation technique of food technology and involves all cultivations of microorganisms on a solid substrate without free liquid phase. In the course of development of Biotechnology it was replaced by liquid cultivation mainly in the western countries. Over the past few years, solid-state fermentation is now becoming more important and has moved more back into focus. Especially, it is suitable for the cultivation of filamentous organisms, like ascomycetes and basidiomycetes, but also for various yeasts and bacteria. The products and applications of solid-state fermentation are as diverse as the microorganisms. They range from enzyme production to the production of antibiotics and pigments to the use in environmental technology and energy production.
Solid State Fermentation for Foods and Beverages (Fermented Foods and Beverages Series #2)
by Jian Chen Yang ZhuAlthough one of the oldest microbial technologies used in food processing, solid-state fermentation (SSF) had, until recently, fallen out of favor. However, based on a series of established mathematical models, new design concepts for SSF bioreactors and process control strategies have been proposed, allowing SSF technology to reach new levels. Sol
Solid State Gas Sensors - Industrial Application
by Maximilian Fleischer Mirko LehmannGas sensor products are very often the key to innovations in the fields of comfort, security, health, environment, and energy savings. This compendium focuses on what the research community labels as solid state gas sensors, where a gas directly changes the electrical properties of a solid, serving as the primary signal for the transducer. It starts with a visionary approach to how life in future buildings can benefit from the power of gas sensors. The requirements for various applications, such as for example the automotive industry, are then discussed in several chapters. Further contributions highlight current trends in new sensing principles, such as the use of nanomaterials and how to use new sensing principles for innovative applications in e.g. meteorology. So as to bring together the views of all the different groups needed to produce new gas sensing applications, renowned industrial and academic representatives report on their experiences and expectations in research, applications and industrialisation.
Solid State Gas Sensors - Industrial Application (Springer Series on Chemical Sensors and Biosensors #11)
by Maximilian Fleischer Mirko LehmannGas sensor products are very often the key to innovations in the fields of comfort, security, health, environment, and energy savings. This compendium focuses on what the research community labels as solid state gas sensors, where a gas directly changes the electrical properties of a solid, serving as the primary signal for the transducer. It starts with a visionary approach to how life in future buildings can benefit from the power of gas sensors. The requirements for various applications, such as for example the automotive industry, are then discussed in several chapters. Further contributions highlight current trends in new sensing principles, such as the use of nanomaterials and how to use new sensing principles for innovative applications in e.g. meteorology. So as to bring together the views of all the different groups needed to produce new gas sensing applications, renowned industrial and academic representatives report on their experiences and expectations in research, applications and industrialisation.
Solid-State Metal Additive Manufacturing: Physics, Processes, Mechanical Properties, and Applications
by Hang Z. Yu Nihan Tuncer Zhili FengSolid-State Metal Additive Manufacturing Timely summary of state-of-the-art solid-state metal 3D printing technologies, focusing on fundamental processing science and industrial applications Solid-State Metal Additive Manufacturing: Physics, Processes, Mechanical Properties, and Applications provides detailed and in-depth discussion on different solid-state metal additive manufacturing processes and applications, presenting associated methods, mechanisms and models, and unique benefits, as well as a detailed comparison to traditional fusion-based metal additive manufacturing. The text begins with a high-level overview of solid-state metal additive manufacturing with an emphasis on its position within the metal additive manufacturing spectrum and its potential for meeting specific demands in the aerospace, automotive, and defense industries. Next, each of the four categories of solid-state additive technologies—cold spray additive manufacturing, additive friction stir deposition, ultrasonic additive manufacturing, and sintering-based processes—is discussed in depth, reviewing advances in processing science, metallurgical science, and innovative applications. Finally, the future directions of these solid-state processes, especially the material innovation and artificial intelligence aspects, are discussed. Sample topics covered in Solid-State Metal Additive Manufacturing include: Physical processes and bonding mechanisms in impact-induced bonding and microstructures and microstructural evolution in cold sprayed materialsProcess fundamentals, dynamic microstructure evolution, and potential industrial applications of additive friction stir depositionMicrostructural and mechanical characterization and industrial applications of ultrasonic additive manufacturingPrinciples of solid-state sintering, binder jetting-based metal printing, and sintering-based metal additive manufacturing methods for magnetic materialsCritical issues inherent to melting and solidification, such as porosity, high residual stress, cast microstructure, anisotropic mechanical properties, and hot cracking Solid-State Metal Additive Manufacturing is an essential reference on the subject for academic researchers in materials science, mechanical, and biomedicine, as well as professional engineers in various manufacturing industries, especially those involved in building new additive technologies.
Solid State Nanopores: From Fabrication to Biosensing (Nanostructure Science and Technology)
by Jean-Pierre LeburtonThis contributed volume provides an overview of the recent advances in solid-state nanopore technology, featuring contributions by leading experts in the field. It discusses several aspects of solid-state nanopores, covering their fabrication as well as multiple biosensing applications. It successfully bridges the gap between various scientific and engineering disciplines and highlights the progress made in this area. This title is a useful tool for acquiring basic knowledge of this field and following recent progress. It is a valuable contribution to the area of nanopore biosensing and is of interest to graduate students, postdocs, or senior researchers working in the fields of physical chemistry, biochemistry, bio- and electrical engineering, and biophysics.
Solid State NMR
by Jerry C. ChanDipolar Recoupling, by Niels Chr. Nielsen, Lasse A. Strassø and Anders B. Nielsen.- Solid-State NMR Techniques for the Structural Determination of Amyloid Fibrils, by Jerry C. C. Chan.- Solid-State 19F-NMR of Peptides in Native Membranes, by Katja Koch, Sergii Afonin, Marco Ieronimo, Marina Berditsch and Anne S. Ulrich.- Probing Quadrupolar Nuclei by Solid-State NMR Spectroscopy: Recent Advances, by Christian Fernandez and Marek Pruski.- Solid State NMR of Porous Materials Zeolites and Related Materials, by Hubert Koller and Mark Weiß.- Solid-State NMR of Inorganic Semiconductors, by James P. Yesinowski.-
Solid State NMR: Principles, Methods, and Applications
by Klaus Müller Marco GeppiSolid State NMR A thorough and comprehensive textbook covering the theoretical background, experimental approaches, and major applications of solid-state NMR spectroscopyNuclear Magnetic Resonance (NMR) spectroscopy is a powerful non-destructive technique capable of providing information about the molecular structure and dynamics of molecules. Alongside solution-state NMR, a well-established technique to study chemical structures and investigate physico-chemical properties of molecules in solutions, solid-state NMR (SSNMR) offers many exciting possibilities for the analysis of solid and soft materials across scientific fields. SSNMR shows unique capabilities for a detailed investigation of structural and dynamic properties of materials over wide space and time ranges. For this reason, and thanks to significant advances in the past several years, the application of SSNMR to materials is rapidly increasing in disciplines such as chemistry, physics, and materials and life sciences.Solid State NMR: Principles, Methods, and Applications offers a systematic introduction to the theory, methodological concepts, and major experimental methods of SSMR spectroscopy. Exploring the unique potential of SSNMR for the structural and dynamic characterization of soft and either amorphous or crystalline solid materials, this comprehensive textbook provides foundational knowledge and recent developments of SSNMR, covering physical and theoretical background, experimental methods, and applications to pharmaceuticals, polymers, inorganic and hybrid materials, liquid crystals, and model membranes. Written by two expert authors to ensure a clear and consistent presentation of the subject, this textbook:Includes a brief introduction to the historical aspects and broad theoretical background of solid-state NMR spectroscopyProvides helpful illustrations to explain the various SSNMR concepts and methodsFeatures accessible descriptive text with self-consistent use of quantum mechanicsCovers the experimental aspects of SSNMR spectroscopy and in particular a description of many useful pulse sequencesContains references to relevant literatureSolid State NMR: Principles, Methods, and Applications is the ideal textbook for university courses on SSNMR, advanced spectroscopies, and a valuable single-volume reference for spectroscopists, chemists, and researchers in the field of materials.
Solid-State NMR in Zeolite Catalysis (Lecture Notes in Chemistry #103)
by Jun Xu Qiang Wang Shenhui Li Feng DengSolid-State NMR Characterization of Heterogeneous Catalysts and Catalytic Reactions provides a comprehensive account of state-of-the-art solid-state NMR techniques and the application of these techniques in heterogeneous catalysts and related catalytic reactions. It includes an introduction to the basic theory of solid-state NMR and various frequently used techniques. Special emphasis is placed on characterizing the framework and pore structure, active site, guest-host interaction, and synthesis mechanisms of heterogeneous catalysts using multinuclear one- and two-dimensional solid-sate NMR spectroscopy. Additionally, various in-situ solid-state NMR techniques and their applications in investigation of the mechanism of industrially important catalytic reactions are also discussed. Both the fundamentals and the latest research results are covered, making the book suitable as a reference guide for both experienced researchers in and newcomers to this field.Feng Deng is a Professor at Wuhan Institute of Physics and Mathematics, Chinese Academy of Sciences.
Solid State NMR Studies of Biopolymers
by Tatyana Polenova Anne E. McdermottThe content of this volume has been added to eMagRes (formerly Encyclopedia of Magnetic Resonance) - the ultimate online resource for NMR and MRI.The field of solid state NMR of biological samples [ssNMR] has blossomed in the past 5-10 years, and a cohesive overview of the technology is needed for new practitioners in industry and academia. This title provides an overview of Solid State NMR methods for studying structure dynamics and ligand-binding in biopolymers, and offers an overview of RF pulse sequences for various applications, including not only a systematic catalog but also a discussion of theoretical tools for analysis of pulse sequences. Practical examples of biochemical applications are included, along with a detailed discussion of the many aspects of sample preparation and handling that make spectroscopy on solid proteins successful.About EMR Handbooks / eMagRes Handbooks The Encyclopedia of Magnetic Resonance (up to 2012) and eMagRes (from 2013 onward) publish a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of EMR Handbooks / eMagRes Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of articles from eMagRes. In consultation with the eMagRes Editorial Board, the EMR Handbooks / eMagRes Handbooks are coherently planned in advance by specially-selected Editors, and new articles are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry.Have the content of this Handbook and the complete content of eMagRes at your fingertips! Visit: www.wileyonlinelibrary.com/ref/eMagResView other eMagRes publications here
Solid State Physics
by Philip HofmannA must-have textbook for any undergraduate studying solid state physics. This successful brief course in solid state physics is now in its second edition. The clear and concise introduction not only describes all the basic phenomena and concepts, but also such advanced issues as magnetism and superconductivity. Each section starts with a gentle introduction, covering basic principles, progressing to a more advanced level in order to present a comprehensive overview of the subject. The book is providing qualitative discussions that help undergraduates understand concepts even if they can't follow all the mathematical detail. The revised edition has been carefully updated to present an up-to-date account of the essential topics and recent developments in this exciting field of physics. The coverage now includes ground-breaking materials with high relevance for applications in communication and energy, like graphene and topological insulators, as well as transparent conductors. The text assumes only basic mathematical knowledge on the part of the reader and includes more than 100 discussion questions and some 70 problems, with solutions free to lecturers from the Wiley-VCH website. The author′s webpage provides Online Notes on x-ray scattering, elastic constants, the quantum Hall effect, tight binding model, atomic magnetism, and topological insulators. This new edition includes the following updates and new features: ∗ Expanded coverage of mechanical properties of solids, including an improved discussion of the yield stress ∗ Crystal structure, mechanical properties, and band structure of graphene ∗ The coverage of electronic properties of metals is expanded by a section on the quantum hall effect including exercises. New topics include the tight-binding model and an expanded discussion on Bloch waves. ∗ With respect to semiconductors, the discussion of solar cells has been extended and improved. ∗ Revised coverage of magnetism, with additional material on atomic magnetism ∗ More extensive treatment of finite solids and nanostructures, now including topological insulators ∗ Recommendations for further reading have been updated and increased. ∗ New exercises on Hall mobility, light penetrating metals, band structure